Information card for entry 4322089

Structure parameters

• Formula: C40 H44 B9 Cl2 Cu O P2 Ru
• Calculated formula: C40 H44 B9 Cl2 Cu O P2 Ru
• Title of publication: The Reagent [K(18-crown-6)][RuH(PPh3)2(η5-7,8-C2B9H11)] as a Precursor to New Ruthenacarborane Complexes
• Authors of publication: Dianne D. Ellis; Samantha M. Couchman; John C. Jeffery; John M. Malget; F. Gordon A. Stone
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2981 - 2988
• a: 17.996 ± 0.005 Å
• b: 13.44 ± 0.003 Å
• c: 19.689 ± 0.006 Å
• α: 90°
• β: 110.41 ± 0.03°
• γ: 90°
• Cell volume: 4463 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1081
• Residual factor for significantly intense reflections: 0.0622
• Weighted residual factors for all reflections: 0.1354
• Weighted residual factors for significantly intense reflections: 0.1203
• Goodness-of-fit parameter for all reflections: 1.136
• Goodness-of-fit parameter for significantly intense reflections: 1.284
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No