Information card for entry 4322115

Structure parameters

• Formula: C63 H56 B2 Cd F24 N12
• Calculated formula: C63 H56 B2 Cd F24 N12
• Title of publication: Solid State Structure of {[HC(3,5-Me2pz)3][HB(3,5-Me2pz)3]Cd}{B[3,5-(CF3)2C6H3]4}: Comparison of the Bonding of Tris(pyrazolyl)methane and Tris(pyrazolyl)borate Ligands
• Authors of publication: Daniel L. Reger; James E. Collins; Arnold L. Rheingold; Louise M. Liable-Sands
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 3235 - 3237
• a: 10.311 ± 0.006 Å
• b: 19.045 ± 0.005 Å
• c: 19.611 ± 0.006 Å
• α: 108.5 ± 0.02°
• β: 96.53 ± 0.05°
• γ: 103.23 ± 0.04°
• Cell volume: 3482 ± 3 ų
• Cell temperature: 244 ± 2 K
• Ambient diffraction temperature: 244 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0953
• Residual factor for significantly intense reflections: 0.0601
• Weighted residual factors for all reflections: 0.1345
• Weighted residual factors for significantly intense reflections: 0.1273
• Goodness-of-fit parameter for all reflections: 1.251
• Goodness-of-fit parameter for significantly intense reflections: 1.557
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No