Information card for entry 4322129

Structure parameters

• Chemical name: Chromium(V)mon-oxo-bis(tert-butyl, 2,5-fluoro-methyl-anilide)triphenylsiloxide.
• Formula: C40 H45 Cr F2 N2 O2 Si
• Calculated formula: C40 H36 Cr F2 N2 O2 Si
• Title of publication: A Nucleophilic Chromium(V) Dioxo Radical Anion
• Authors of publication: Aaron L. Odom; Daniel J. Mindiola; Christopher C. Cummins
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 3290 - 3295
• a: 9.6227 ± 0.0009 Å
• b: 10.3127 ± 0.001 Å
• c: 19.649 ± 0.002 Å
• α: 80.855 ± 0.002°
• β: 81.889 ± 0.002°
• γ: 72.625 ± 0.002°
• Cell volume: 1828.2 ± 0.3 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1123
• Residual factor for significantly intense reflections: 0.0887
• Weighted residual factors for all reflections: 0.195
• Weighted residual factors for significantly intense reflections: 0.1745
• Goodness-of-fit parameter for all reflections: 1.171
• Goodness-of-fit parameter for significantly intense reflections: 1.218
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No