Information card for entry 4322141

Structure parameters

• Chemical name: trans-Tetrachloro-bis(triethylphosphine)-rhenium (IV)
• Formula: C12 H30 Cl4 P2 Re
• Calculated formula: C12 H30 Cl4 P2 Re
• SMILES: C(C)[P](CC)(CC)[Re](Cl)(Cl)([P](CC)(CC)CC)(Cl)Cl
• Title of publication: Mixed Chloride/Phosphine Complexes of the Dirhenium Core. 5. Reduction or Disproportionation at the Re26+ Unit in Reactions with Tertiary Phosphines in Different Solvents
• Authors of publication: F. Albert Cotton; Evgeny V. Dikarev; Marina A. Petrukhina
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 3384 - 3389
• a: 12.876 ± 0.002 Å
• b: 12.1351 ± 0.0007 Å
• c: 13.2125 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2064.5 ± 0.4 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0401
• Residual factor for significantly intense reflections: 0.0333
• Weighted residual factors for all reflections: 0.087
• Weighted residual factors for significantly intense reflections: 0.0817
• Goodness-of-fit parameter for all reflections: 1.092
• Goodness-of-fit parameter for significantly intense reflections: 1.126
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No