Information card for entry 4322143

Structure parameters

• Chemical name: Pentachloro-tris(tripropylphosphine)-di-rhenium (II,III), 1,3,6-isomer
• Formula: C27 H63 Cl5 P3 Re2
• Calculated formula: C27 H63 Cl5 P3 Re2
• Title of publication: Mixed Chloride/Phosphine Complexes of the Dirhenium Core. 5. Reduction or Disproportionation at the Re26+ Unit in Reactions with Tertiary Phosphines in Different Solvents
• Authors of publication: F. Albert Cotton; Evgeny V. Dikarev; Marina A. Petrukhina
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 3384 - 3389
• a: 12.214 ± 0.002 Å
• b: 15.296 ± 0.002 Å
• c: 20.945 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3913.1 ± 1.4 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0661
• Residual factor for significantly intense reflections: 0.0526
• Weighted residual factors for all reflections: 0.1313
• Weighted residual factors for significantly intense reflections: 0.1231
• Goodness-of-fit parameter for all reflections: 1.091
• Goodness-of-fit parameter for significantly intense reflections: 1.086
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No