Information card for entry 4322145

Structure parameters

• Formula: C29 H27 P Re S3
• Calculated formula: C29 H27 P Re S3
• Title of publication: Synthesis and Structural Characterization of Novel Terminal and Bridging Re(V)-Sulfido Complexes
• Authors of publication: Josemon Jacob; Ilia A. Guzei; James H. Espenson
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 3266 - 3267
• a: 9.2936 ± 0.0005 Å
• b: 22.2088 ± 0.0012 Å
• c: 13.0576 ± 0.0007 Å
• α: 90°
• β: 91.237 ± 0.001°
• γ: 90°
• Cell volume: 2694.5 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0408
• Residual factor for significantly intense reflections: 0.0246
• Weighted residual factors for significantly intense reflections: 0.0416
• Weighted residual factors for all reflections included in the refinement: 0.0436
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No