Information card for entry 4322168

Structure parameters

• Formula: C44.9 H29.8 Cl2.8 Mo N4 O5
• Calculated formula: C44.9 H28 Cl2.8 Mo N4 O5
• Title of publication: Molybdenum(V) on an Oxide String. Synthesis and Structure of the Novel Linear Trinuclear Complex {[MoO(TPP)][O-Mo(TPP)-O][MoO(TPP)]}ClO4
• Authors of publication: Brent J. Hamstra; Beisong Cheng; Mary K. Ellison; W. Robert Scheidt
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 3554 - 3561
• a: 11.437 ± 0.002 Å
• b: 13.537 ± 0.006 Å
• c: 13.764 ± 0.004 Å
• α: 89.15 ± 0.01°
• β: 108.86 ± 0.01°
• γ: 103.96 ± 0.02°
• Cell volume: 1952.4 ± 1.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0496
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for all reflections: 0.1124
• Weighted residual factors for significantly intense reflections: 0.1082
• Goodness-of-fit parameter for all reflections: 1.079
• Goodness-of-fit parameter for significantly intense reflections: 1.101
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No