Information card for entry 4322196

Structure parameters

• Chemical name: Salben{B(OSiPh3)2}2
• Formula: C59 H56 B N O3 Si2
• Calculated formula: C59 H53 B N O3 Si2
• Title of publication: Synthesis and Structures of Salen-Supported Borates Containing Siloxides
• Authors of publication: Pingrong Wei; Timothy Keizer; David A. Atwood
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 3914 - 3918
• a: 13.8621 ± 0.0011 Å
• b: 14.0457 ± 0.001 Å
• c: 15.2496 ± 0.0011 Å
• α: 82.367 ± 0.001°
• β: 80.105 ± 0.001°
• γ: 62.32 ± 0.001°
• Cell volume: 2585.4 ± 0.3 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0742
• Residual factor for significantly intense reflections: 0.0602
• Weighted residual factors for all reflections: 0.1709
• Weighted residual factors for significantly intense reflections: 0.1531
• Goodness-of-fit parameter for all reflections: 1
• Goodness-of-fit parameter for significantly intense reflections: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No