Information card for entry 4322212

Structure parameters

• Formula: C48 H52 La N3 O20
• Calculated formula: C48 H30 La N3 O20
• Title of publication: Lanthanide Complexes of 3-Diphenylamino-4-hydroxycyclobut-3-ene-1,2-dione (Diphenylaminosquarate)
• Authors of publication: Bert D. Alleyne; Leonard St. Bernard; Hema Jaggernauth; Lincoln A. Hall; Ian Baxter; Andrew J. P. White; David J. Williams
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 3774 - 3778
• a: 9.2791 ± 0.0013 Å
• b: 13.371 ± 0.003 Å
• c: 20.137 ± 0.003 Å
• α: 95.145 ± 0.013°
• β: 97.282 ± 0.01°
• γ: 92.32 ± 0.02°
• Cell volume: 2464.9 ± 0.8 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1091
• Residual factor for significantly intense reflections: 0.0819
• Weighted residual factors for all reflections: 0.2248
• Weighted residual factors for significantly intense reflections: 0.1982
• Goodness-of-fit parameter for all reflections: 1.063
• Goodness-of-fit parameter for significantly intense reflections: 1.082
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No