Information card for entry 4322222

Structure parameters

• Chemical name: Hexachloro-bis(tripropylphosphine)-di-rhenium (II, III), 1,6-isomer, terabutylammonium salt
• Formula: C34 H78 Cl6 N P2 Re2
• Calculated formula: C34 H78 Cl6 N P2 Re2
• Title of publication: Mixed Chloride/Phosphine Complexes of the Dirhenium Core. 6. Rare or Unprecedented Isomers of [Re2Cl6(PR3)2] Stoichiometry
• Authors of publication: F. Albert Cotton; Evgeny V. Dikarev; Marina A. Petrukhina
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 3889 - 3894
• a: 16.3355 ± 0.0008 Å
• b: 12.656 ± 0.001 Å
• c: 22.892 ± 0.002 Å
• α: 90°
• β: 94.735 ± 0.006°
• γ: 90°
• Cell volume: 4716.6 ± 0.6 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0499
• Residual factor for significantly intense reflections: 0.0451
• Weighted residual factors for all reflections: 0.1007
• Weighted residual factors for significantly intense reflections: 0.097
• Goodness-of-fit parameter for all reflections: 1.206
• Goodness-of-fit parameter for significantly intense reflections: 1.212
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No