Information card for entry 4322256

Structure parameters

• Formula: C112 H232 Cl8 N32 Ni8 O44 S8
• Calculated formula: C28 H58 Cl2 N8 Ni2 O11 S2
• Title of publication: Coordination and Conversion of Urea at Dinuclear μ-Acetato Nickel(II) Complexes with Symmetric and Asymmetric Cores
• Authors of publication: Matthias Konrad; Franc Meyer; Albrecht Jacobi; Peter Kircher; Peter Rutsch; Laszlo Zsolnai
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 4559 - 4566
• a: 13.932 ± 0.003 Å
• b: 18.748 ± 0.004 Å
• c: 15.517 ± 0.003 Å
• α: 90°
• β: 91.07 ± 0.03°
• γ: 90°
• Cell volume: 4052.3 ± 1.5 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1792
• Residual factor for significantly intense reflections: 0.0582
• Weighted residual factors for significantly intense reflections: 0.1295
• Weighted residual factors for all reflections included in the refinement: 0.162
• Goodness-of-fit parameter for all reflections included in the refinement: 0.854
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No