Information card for entry 4322368

Structure parameters

• Formula: C42 H84 K4 O10 Sn2
• Calculated formula: C10.485 K O2.5 Sn0.5
• Title of publication: Unusual Sandwiching of the Cyclopentadienyl Anion in [K4(C5H5)2M2(OBut)6(CH3OCH2CH2OCH3)2]n (M = Ge, Sn)
• Authors of publication: Michael Veith; Charu Mathur; Sanjay Mathur; Volker Huch
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 5461 - 5463
• a: 9.907 ± 0.002 Å
• b: 10.722 ± 0.002 Å
• c: 14.162 ± 0.003 Å
• α: 81.95 ± 0.03°
• β: 89.62 ± 0.03°
• γ: 82.69 ± 0.03°
• Cell volume: 1477.3 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0543
• Residual factor for significantly intense reflections: 0.046
• Weighted residual factors for significantly intense reflections: 0.1339
• Weighted residual factors for all reflections included in the refinement: 0.1396
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No