Information card for entry 4322396

Structure parameters

• Formula: C40.75 H55.75 N3 O4 Ru S2 Si4 Zr
• Calculated formula: C40.75 H55.75 N3 O4 Ru S2 Si4 Zr
• Title of publication: Synthesis and Reactivity of Early-Late Heterodinuclear Complexes Stabilized by a Trisilylsilane-Based Tripodal Amido Ligand
• Authors of publication: Lutz H. Gade; Martin Schubart; Bernd Findeis; Sylvie Fabre; Izoldi Bezougli; Matthias Lutz; Ian J. Scowen; Mary McPartlin
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 5282 - 5294
• a: 12.426 ± 0.003 Å
• b: 14.51 ± 0.003 Å
• c: 16.742 ± 0.004 Å
• α: 115.406 ± 0.017°
• β: 96.302 ± 0.013°
• γ: 96.682 ± 0.015°
• Cell volume: 2664.9 ± 1.2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1602
• Residual factor for significantly intense reflections: 0.0705
• Weighted residual factors for significantly intense reflections: 0.1505
• Weighted residual factors for all reflections included in the refinement: 0.1758
• Goodness-of-fit parameter for all reflections included in the refinement: 0.953
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No