Information card for entry 4322399

Structure parameters

• Formula: C48 H53 N23.5 Ni4 O24.5
• Calculated formula: C48 H53 N23.5 Ni4 O24.5
• Title of publication: Tetranuclear Copper(II) and Nickel(II) Cluster Complexes Derived by Self-Assembly from a Series of Tetradentate Diazine Ligands: Structural and Magnetic Studies
• Authors of publication: Craig J. Matthews; Karen Avery; Zhiqiang Xu; Laurence K. Thompson; Liang Zhao; David O. Miller; Kumar Biradha; Karen Poirier; Michael J. Zaworotko; Claire Wilson; Andrés E. Goeta; Judith A. K. Howard
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 5266 - 5276
• a: 12.0509 ± 0.0006 Å
• b: 12.7498 ± 0.0006 Å
• c: 23.1208 ± 0.0011 Å
• α: 93.105 ± 0.001°
• β: 100.15 ± 0.001°
• γ: 108.505 ± 0.001°
• Cell volume: 3292.9 ± 0.3 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0871
• Residual factor for significantly intense reflections: 0.0659
• Weighted residual factors for all reflections: 0.2171
• Weighted residual factors for significantly intense reflections: 0.1992
• Goodness-of-fit parameter for all reflections: 1.03
• Goodness-of-fit parameter for significantly intense reflections: 1.086
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No