Information card for entry 4322416

Structure parameters

• Chemical name: di-[(N,N'-ethylenebis(salicylideneiminato)nickel(ii)]-di-aquo-nickel(ii)perc hlorate
• Formula: C32 H32 Cl2 N4 Ni3 O14
• Calculated formula: C32 H32 Cl2 N4 Ni3 O14
• Title of publication: Spectrophotometric Study of the Equilibria between Nickel(II) Schiff-Base Complexes and Alkaline Earth or Nickel(II) Cations in Acetonitrile Solution
• Authors of publication: Laura Carbonaro; Mauro Isola; Piero La Pegna; Lucio Senatore; Fabio Marchetti
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 5519 - 5525
• a: 10.302 ± 0.0015 Å
• b: 21.818 ± 0.003 Å
• c: 17.796 ± 0.004 Å
• α: 90°
• β: 118.98 ± 0.02°
• γ: 90°
• Cell volume: 3499.1 ± 1.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1186
• Residual factor for significantly intense reflections: 0.065
• Weighted residual factors for significantly intense reflections: 0.1396
• Weighted residual factors for all reflections included in the refinement: 0.165
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No