Information card for entry 4322453

Structure parameters

• Formula: C24 H40 F12 N2 O S4 W
• Calculated formula: C24 H40 F12 N2 O S4 W
• Title of publication: Syntheses of Metal Dithiolene Complexes from Thiometalates by Induced Internal Redox Reactions
• Authors of publication: Kun Wang; Jonathan M. McConnachie; Edward I. Stiefel
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 4334 - 4341
• a: 12.2 ± 0.002 Å
• b: 18.63 ± 0.004 Å
• c: 15.463 ± 0.003 Å
• α: 90°
• β: 91.02 ± 0.03°
• γ: 90°
• Cell volume: 3514 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0757
• Residual factor for significantly intense reflections: 0.0456
• Weighted residual factors for all reflections: 0.1067
• Weighted residual factors for significantly intense reflections: 0.093
• Goodness-of-fit parameter for all reflections: 1.09
• Goodness-of-fit parameter for significantly intense reflections: 1.127
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No