Information card for entry 4322466

Structure parameters

• Formula: C17 H20 B Cl2 N6 O2 Re
• Calculated formula: C17 H20 B Cl2 N6 O2 Re
• Title of publication: Rhenium(V) Dioxo Complexes with Dihydrobis(pyrazolyl)borates: Synthesis and Reactivity toward Electrophilic Substrates
• Authors of publication: K. Rajender Reddy; Ângela Domingos; António Paulo; Isabel Santos
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 4278 - 4282
• a: 9.419 ± 0.001 Å
• b: 9.584 ± 0.001 Å
• c: 12.652 ± 0.001 Å
• α: 89.03 ± 0.01°
• β: 82.41 ± 0.01°
• γ: 72.75 ± 0.01°
• Cell volume: 1080.89 ± 0.19 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0476
• Residual factor for significantly intense reflections: 0.0313
• Weighted residual factors for all reflections: 0.0798
• Weighted residual factors for significantly intense reflections: 0.0674
• Goodness-of-fit parameter for all reflections: 1.169
• Goodness-of-fit parameter for significantly intense reflections: 1.153
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No