Information card for entry 4322594

Structure parameters

• Formula: C60 H74 Cu6 N3 P S11 W3
• Calculated formula: C60 H29 Cu6 N3 P S11 W3
• Title of publication: Assembly of Three WS3Cu2 Cluster Units by μ3-S Bridges: Synthesis of [PPh4][{(C5Me5)WS3Cu2}3S2]
• Authors of publication: Jian-Ping Lang; Kazuyuki Tatsumi
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 160 - 162
• a: 15.477 ± 0.004 Å
• b: 21.652 ± 0.005 Å
• c: 21.623 ± 0.002 Å
• α: 90°
• β: 91.35 ± 0.01°
• γ: 90°
• Cell volume: 7244 ± 3 ų
• Cell temperature: 296.2 K
• Ambient diffraction temperature: 296.2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0487
• Weighted residual factors for significantly intense reflections: 0.0552
• Goodness-of-fit parameter for significantly intense reflections: 1.63
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No