Information card for entry 4322618

Structure parameters

• Formula: C15 H34 Cl Cu N7 Ni O7 S
• Calculated formula: C15 H33 Cl Cu N7 Ni O7 S
• Title of publication: Synthesis and Magnetic Properties of Four New (Cu-Ni)2 Tetranuclear Complexes of General Formula [Cu(oxpn)Ni(μ-NCS)(H2O)(aa)]2(X)2 (oxpn =N,N'-Bis(3-aminopropyl)oxamide; aa = Bidentate Amine; X = ClO4- or PF6-). Ferro- and Antiferromagnetic Alternation
• Authors of publication: Joan Ribas; Carmen Diaz; Ramon Costa; Javier Tercero; Xavier Solans; Mercé Font-Bardía; Helen Stoeckli-Evans
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 233 - 239
• a: 8.7586 ± 0.0007 Å
• b: 12.58 ± 0.004 Å
• c: 12.6318 ± 0.0012 Å
• α: 94.63 ± 0.014°
• β: 98.485 ± 0.008°
• γ: 107.963 ± 0.013°
• Cell volume: 1297.6 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0716
• Residual factor for significantly intense reflections: 0.0398
• Weighted residual factors for all reflections: 0.1752
• Weighted residual factors for significantly intense reflections: 0.1107
• Goodness-of-fit parameter for all reflections: 0.689
• Goodness-of-fit parameter for significantly intense reflections: 0.583
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No