Information card for entry 4322701

Structure parameters

• Formula: C18 H22 B Br4 N7 O W
• Calculated formula: C17.793 H21.793 B Br4 N6.931 O0.931 W
• Title of publication: Halocarbonyltungsten(II) Complexes Containing Tripodal Tris(pyrazolyl)borate Ligands
• Authors of publication: Charles G. Young; Simon Thomas; Robert W. Gable
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 1299 - 1306
• a: 22.245 ± 0.004 Å
• b: 19.077 ± 0.004 Å
• c: 15.639 ± 0.003 Å
• α: 90°
• β: 128.61 ± 0.02°
• γ: 90°
• Cell volume: 5186 ± 2 ų
• Cell temperature: 293 ± 1 K
• Ambient diffraction temperature: 293 ± 1 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0862
• Residual factor for significantly intense reflections: 0.0515
• Weighted residual factors for all reflections: 0.1207
• Weighted residual factors for significantly intense reflections: 0.1061
• Goodness-of-fit parameter for all reflections: 1.04
• Goodness-of-fit parameter for significantly intense reflections: 1.115
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No