Information card for entry 4322703

Structure parameters

• Formula: C57 H53 B D21 F15 N3 Si6 U
• Calculated formula: C57 H53 B D21 F15 N3 Si6 U
• Title of publication: Syntheses of the Uranium Complexes [U{N(SiMe3)2}2{N(SiMe3)(SiMe2CH2B(C6F5)3)}] and [U{C(Ph)(NSiMe3)2}2{μ3-BH4}2]. Determination of Hydrogen Positions by Single-Crystal X-ray and Neutron Diffraction
• Authors of publication: Matthias Müller; V. Cliff Williams; Linda H. Doerrer; Michael A. Leech; Sax A. Mason; Malcolm L. H. Green; Keith Prout
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 1315 - 1323
• a: 13.9927 ± 0.0005 Å
• b: 14.4838 ± 0.0006 Å
• c: 18.7195 ± 0.0006 Å
• α: 82.81 ± 0.002°
• β: 74.12 ± 0.002°
• γ: 63.054 ± 0.002°
• Cell volume: 3252.9 ± 0.2 ų
• Cell temperature: 20 K
• Ambient diffraction temperature: 20 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0748
• Weighted residual factors for significantly intense reflections: 0.07
• Goodness-of-fit parameter for significantly intense reflections: 1.1781
• Diffraction radiation probe: neutron
• Diffraction radiation wavelength: 1.5394 Å
• Diffraction radiation type: thermalneutrons
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes