Information card for entry 4322808

Structure parameters

• Chemical name: (1,4-bis(diphenylphosphino)buthane)palladium(II)(m-buthanodithiolate) (1,5-cyclooctadiene)rhodium(I)perchlorate
• Formula: C40.5 H48 Cl2 O4 P2 Pd Rh S2
• Calculated formula: C40.5 H48 Cl2 O4 P2 Pd Rh S2
• Title of publication: Mononuclear Platinum(II) and Palladium(II) Dithiolate Complexes as Chelate Metalloligands for Preparation of Heterobimetallic d8-d8 Complexes
• Authors of publication: Jorge Forniés-Cámer; Anna M. Masdeu-Bultó; Carmen Claver; Christine J. Cardin
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 2626 - 2632
• a: 20.365 ± 0.006 Å
• b: 14.186 ± 0.006 Å
• c: 14.592 ± 0.006 Å
• α: 90°
• β: 101.04 ± 0.06°
• γ: 90°
• Cell volume: 4138 ± 3 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0745
• Residual factor for significantly intense reflections: 0.0507
• Weighted residual factors for all reflections: 0.1745
• Weighted residual factors for significantly intense reflections: 0.15
• Goodness-of-fit parameter for all reflections: 1.027
• Goodness-of-fit parameter for significantly intense reflections: 1.056
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No