Information card for entry 4322883

Structure parameters

• Formula: C8.33 H10.67 Cl0.67 N5.33 Ni0.67 O5.33
• Calculated formula: C8.33333 H10.6667 Cl0.666667 N5.33333 Ni0.666667 O5.36
• Title of publication: Spiral Dinuclear Complexes of Tetradentate N4 Diazine Ligands with Mn(II), Fe(II), Fe(III), Co(III), and Ni(II) Salts
• Authors of publication: Zhiqiang Xu; Laurence K. Thompson; David O. Miller; Howard J. Clase; Judith A. K. Howard; Andrés E. Goeta
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 3620 - 3627
• a: 17.373 ± 0.003 Å
• b: 17.373 ± 0.003 Å
• c: 33.235 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 8687 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 167
• Hermann-Mauguin space group symbol: R -3 c :H
• Hall space group symbol: -R 3 2"c
• Residual factor for all reflections: 0.0488
• Residual factor for significantly intense reflections: 0.0404
• Weighted residual factors for all reflections: 0.1269
• Weighted residual factors for significantly intense reflections: 0.1124
• Goodness-of-fit parameter for all reflections: 1.124
• Goodness-of-fit parameter for significantly intense reflections: 1.111
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No