Information card for entry 4322900

Structure parameters

• Formula: C10 H26 O P Rb Si2
• Calculated formula: C10 H26 O P Rb Si2
• Title of publication: A Convenient Synthetic Strategy toward Heavy Alkali Metal Bis(trimethylsilyl)phosphides: Crystal Structures of the Ladder-Type Polymers [A(thf)P(SiMe3)2]∞(A = K, Rb, Cs)
• Authors of publication: Ulrich Englich; Karl Hassler; Karin Ruhlandt-Senge; Frank Uhlig
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 3532 - 3537
• a: 6.5338 ± 0.0002 Å
• b: 12.5664 ± 0.0003 Å
• c: 21.5537 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1769.7 ± 0.08 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0776
• Residual factor for significantly intense reflections: 0.0554
• Weighted residual factors for all reflections: 0.1309
• Weighted residual factors for significantly intense reflections: 0.1223
• Goodness-of-fit parameter for all reflections: 0.975
• Goodness-of-fit parameter for significantly intense reflections: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No