Crystallography Open Database

Information card for entry 4322950

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Coordinates	4322950.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C56 H140 Mo6 O66 S16 Sb
Calculated formula	C56 Mo6 O66 S16 Sb
Title of publication	Sulfur-Bridged Sandwich Cubane-Type Molybdenum-Antimony Cluster. Synthesis, X-ray Structure, and 121Sb Mössbauer Spectra of [(H2O)9Mo3S4SbS4Mo3(H2O)9](CH3C6H4SO3)8.24H2O
Authors of publication	Genta Sakane; Kouichi Hashimoto; Masashi Takahashi; Masuo Takeda; Takashi Shibahara
Journal of publication	Inorganic Chemistry
Year of publication	1998
Journal volume	37
Pages of publication	4231 - 4234
a	14.468 ± 0.003 Å
b	18.531 ± 0.005 Å
c	13.713 ± 0.006 Å
α	105.26 ± 0.02°
β	119.71 ± 0.01°
γ	72.48 ± 0.03°
Cell volume	3016.1 ± 1.7 Å³
Cell temperature	298.2 K
Ambient diffraction temperature	298.2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0
Residual factor for significantly intense reflections	0
Weighted residual factors for significantly intense reflections	0
Weighted residual factors for all reflections included in the refinement	0.0747
Goodness-of-fit parameter for all reflections included in the refinement	1.332
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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