Information card for entry 4323071

Structure parameters

• Formula: C12 H24 Ag I7 S6
• Calculated formula: C12 H24 Ag I7 S6
• Title of publication: Silver-Thioether Crown Complexes as Templates for the Synthesis of Extended Polyiodide Networks: Synthesis and X-ray Crystal Structures of [Ag2([15]aneS5)2]I12, [Ag([18]aneS6)]I7, [Ag([18]aneS6)]I3, and [Ag([9]aneS3)2]I5
• Authors of publication: Alexander J. Blake; Robert O. Gould; Wan-Sheung Li; Vito Lippolis; Simon Parsons; Christian Radek; Martin Schröder
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 5070 - 5077
• a: 9.458 ± 0.004 Å
• b: 9.458 ± 0.004 Å
• c: 9.458 ± 0.004 Å
• α: 103.79 ± 0.02°
• β: 103.79 ± 0.02°
• γ: 103.79 ± 0.02°
• Cell volume: 757.9 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 166
• Hermann-Mauguin space group symbol: R -3 m :R
• Hall space group symbol: -P 3* 2
• Residual factor for all reflections: 0.0206
• Residual factor for significantly intense reflections: 0.0192
• Weighted residual factors for all reflections: 0.039
• Weighted residual factors for significantly intense reflections: 0.0334
• Goodness-of-fit parameter for all reflections: 1.112
• Goodness-of-fit parameter for significantly intense reflections: 1.12
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKa
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No