Information card for entry 4323108

Structure parameters

• Formula: C66 H66 Mn4 N8 O16
• Calculated formula: C132 H96 Mn8 N16 O32
• Title of publication: Synthesis, Magnetic Properties, and Incomplete Double-Cubane Structure of Manganese(III)-Metal(II) Complexes [Mn(MeOH)L(OH)M(bpy)]2 (M = Zn, Cu, Ni, and Mn; H4L = 1,2-Bis(2-hydroxybenzamido)benzene; bpy = 2,2'-Bipyridine)
• Authors of publication: Yukinari Sunatsuki; Hiromitsu Shimada; Toshihiro Matsuo; Masaaki Nakamura; Fumiaki Kai; Naohide Matsumoto; Nazzareno Re
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 5566 - 5574
• a: 12.511 ± 0.002 Å
• b: 21.129 ± 0.003 Å
• c: 12.811 ± 0.001 Å
• α: 90°
• β: 110.122 ± 0.01°
• γ: 90°
• Cell volume: 3179.8 ± 0.8 ų
• Cell temperature: 20 K
• Ambient diffraction temperature: 20 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.067
• Weighted residual factors for significantly intense reflections: 0.072
• Goodness-of-fit parameter for significantly intense reflections: 2.23
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No