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Information card for entry 4323161
Preview
Coordinates | 4323161.cif |
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Original paper (by DOI) | HTML |
Formula | C79 H66 Cl6 O10 P4 Pd2 |
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Calculated formula | C79 H64 Cl6 O10 P4 Pd2 |
Title of publication | Synthesis and Structure of PdII Complexes Containing the C,C-Chelating Bis-Ylide Ligand [Ph3PC(H)]2CO. X-ray Crystal Structure of {Pd(μ-Cl){[C(H)PPh3]2CO}}2(ClO4)2.CH2Cl2 |
Authors of publication | Larry R. Falvello; Susana Fernández; Rafael Navarro; Angel Rueda; Esteban P. Urriolabeitia |
Journal of publication | Inorganic Chemistry |
Year of publication | 1998 |
Journal volume | 37 |
Pages of publication | 6007 - 6013 |
a | 19.247 ± 0.005 Å |
b | 19.521 ± 0.004 Å |
c | 19.757 ± 0.004 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 7423 ± 3 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 6 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.105 |
Residual factor for significantly intense reflections | 0.0579 |
Weighted residual factors for significantly intense reflections | 0.1223 |
Weighted residual factors for all reflections included in the refinement | 0.1413 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.036 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4323161.html
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