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Information card for entry 4323165
Preview
Coordinates | 4323165.cif |
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Original paper (by DOI) | HTML |
Formula | C41 H57 Li N4 O |
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Calculated formula | C41 H57 Li N4 O |
Title of publication | The Intra- and Intermolecular Oxidative Coupling of Ni(II)-meso-Octaethyl Mono(pyridine)-Tris(pyrrole) Complex Leading to CC Bonds: Pathways to Oligomeric Porphyrinogens |
Authors of publication | Raffaella Crescenzi; Euro Solari; Carlo Floriani; Angiola Chiesi-Villa; Corrado Rizzoli |
Journal of publication | Inorganic Chemistry |
Year of publication | 1998 |
Journal volume | 37 |
Pages of publication | 6044 - 6051 |
a | 11.815 ± 0.002 Å |
b | 15.94 ± 0.03 Å |
c | 11.26 ± 0.02 Å |
α | 99.07 ± 0.02° |
β | 113.88 ± 0.03° |
γ | 71.87 ± 0.02° |
Cell volume | 1842 ± 5 Å3 |
Cell temperature | 25 K |
Ambient diffraction temperature | 143 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1551 |
Residual factor for significantly intense reflections | 0.0636 |
Weighted residual factors for all reflections | 0.2309 |
Weighted residual factors for significantly intense reflections | 0.1705 |
Goodness-of-fit parameter for all reflections | 1.074 |
Goodness-of-fit parameter for significantly intense reflections | 1.214 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKa |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4323165.html
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Users of the data should acknowledge the original authors of the
structural data.