Information card for entry 4323238

Structure parameters

• Common name: [Fe~4~(μ-O)~2~(μ-BMDP)~2~(μ-OAc)~2~][NO~3~]~3~[OH]^.^12H~2~O
• Formula: C66 H89 Fe4 N19 O30
• Calculated formula: C66 H76 Fe4 N19 O30
• Title of publication: Novel Square Arrangements in Tetranuclear and Octanuclear Iron(III) Complexes with Asymmetric Iron Environments Created by the Unsymmetric Bridging Ligand N,N,N'-Tris((N-methyl)-2-benzimidazolylmethyl)-N'-methyl-1,3-diamino-2-propanol
• Authors of publication: Joe H. Satcher,; Marilyn M. Olmstead; Michael W. Droege; Sean R. Parkin; Bruce C. Noll; Leopold May; Alan L. Balch
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 6751 - 6758
• a: 12.228 ± 0.003 Å
• b: 13.915 ± 0.003 Å
• c: 14.12 ± 0.003 Å
• α: 115.99 ± 0.02°
• β: 108.02 ± 0.02°
• γ: 95.73 ± 0.02°
• Cell volume: 1974.2 ± 1 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1024
• Residual factor for significantly intense reflections: 0.0708
• Weighted residual factors for all reflections: 0.225
• Weighted residual factors for significantly intense reflections: 0.1802
• Goodness-of-fit parameter for all reflections: 1.036
• Goodness-of-fit parameter for significantly intense reflections: 1.059
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No