Information card for entry 4323260

Structure parameters

• Formula: C32 H72 Mo2 P4 Si4
• Calculated formula: C32 H72 Mo2.0002 P4 Si4
• Title of publication: Molecular Structures, Vibrational Spectroscopy, and Normal-Mode Analysis of M2(C\τbCR)4(PMe3)4 Dimetallatetraynes. Observation of Strongly Mixed Metal-Metal and Metal-Ligand Vibrational Modes
• Authors of publication: Kevin D. John; Vincent M. Miskowski; Michael A. Vance; Richard F. Dallinger; Louis C. Wang; Steven J. Geib; Michael D. Hopkins
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 6858 - 6873
• a: 19.55 ± 0.005 Å
• b: 18.346 ± 0.005 Å
• c: 14.473 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5191 ± 2 ų
• Cell temperature: 208 ± 2 K
• Ambient diffraction temperature: 208 ± 2 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0774
• Residual factor for significantly intense reflections: 0.0444
• Weighted residual factors for all reflections: 0.1187
• Weighted residual factors for significantly intense reflections: 0.0913
• Goodness-of-fit parameter for all reflections: 1.011
• Goodness-of-fit parameter for significantly intense reflections: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No