Information card for entry 4323290

Structure parameters

• Formula: C57.5 H54 B Br Cl F5 N2 O2 P4 W
• Calculated formula: C230 H216 B4 Br4 Cl4 F20 N8 O8 P16 W4
• Title of publication: Synthesis and Structure Determinations of Complexes Containing a Five-Membered Lactam Structure Based on Organohydrazido(2-) Ligands1
• Authors of publication: Hidetake Seino; Youichi Ishii; Masanobu Hidai
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 161 - 171
• a: 12.798 ± 0.002 Å
• b: 27.619 ± 0.002 Å
• c: 17.002 ± 0.002 Å
• α: 90°
• β: 109.787 ± 0.01°
• γ: 90°
• Cell volume: 5654.8 ± 1.2 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 10
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.049
• Weighted residual factors for significantly intense reflections: 0.033
• Goodness-of-fit parameter for significantly intense reflections: 2.47
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No