Information card for entry 4323292

Structure parameters

• Formula: C13 N15 O49 P Rh2 S2 W11
• Calculated formula: C13 N15 O49 P Rh2 S2 W11
• Title of publication: New Routes for Multiple Derivatization of Polyoxometalates. Bis(acetato)dirhodium-11-tungstophosphate, [(PO4)W11O35{Rh2(OAc)2}]5-
• Authors of publication: Xinyi Wei; Michael H. Dickman; Michael T. Pope
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 130 - 131
• a: 22.451 ± 0.003 Å
• b: 11.8408 ± 0.0014 Å
• c: 25.698 ± 0.003 Å
• α: 90°
• β: 110.833 ± 0.008°
• γ: 90°
• Cell volume: 6384.9 ± 1.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0526
• Residual factor for significantly intense reflections: 0.0468
• Weighted residual factors for all reflections: 0.1146
• Weighted residual factors for significantly intense reflections: 0.1119
• Goodness-of-fit parameter for all reflections: 1.103
• Goodness-of-fit parameter for significantly intense reflections: 1.121
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No