Information card for entry 4323314

Structure parameters

• Chemical name: Tris(tetrahydrofuran)barium = bis[1,3-bis(trimethylsilyl)-2-phenyl-1-aza-3-phosphapropenide]
• Formula: C38 H70 Ba N2 O3 P2 Si4
• Calculated formula: C38 H70 Ba N2 O3 P2 Si4
• Title of publication: 1,3-Bis(trimethylsilyl)-2-phenyl-1-aza-3-phosphapropenide Anions as Bidentate Ligands for the Alkaline Earth Metals Magnesium, Calcium, Strontium, and Barium
• Authors of publication: Matthias Westerhausen; Matthias H. Digeser; Wolfgang Schwarz
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 521 - 527
• a: 12.452 ± 0.004 Å
• b: 19.071 ± 0.004 Å
• c: 22.123 ± 0.007 Å
• α: 76.46 ± 0.02°
• β: 76.45 ± 0.02°
• γ: 89.31 ± 0.02°
• Cell volume: 4960 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0946
• Residual factor for significantly intense reflections: 0.059
• Weighted residual factors for all reflections: 0.1489
• Weighted residual factors for significantly intense reflections: 0.1309
• Goodness-of-fit parameter for all reflections: 1.298
• Goodness-of-fit parameter for significantly intense reflections: 1.401
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No