Information card for entry 4323345

Structure parameters

• Formula: C39 H84 Cl2 Gd2 N4 O2 Si4
• Calculated formula: C39 H84 Cl2 Gd2 N4 O2 Si4
• Title of publication: Novel Cyclopentadienyl-Free Organolanthanides: The First Examples of Five-Membered Amidolanthanide Heterocycles
• Authors of publication: Syed A. A. Shah; Hendrik Dorn; Herbert W. Roesky; Paolo Lubini; Hans-Georg Schmidt
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 1102 - 1106
• a: 10.321 ± 0.002 Å
• b: 11.116 ± 0.002 Å
• c: 13.434 ± 0.003 Å
• α: 107.57 ± 0.03°
• β: 111.31 ± 0.03°
• γ: 90.67 ± 0.03°
• Cell volume: 1356 ± 0.6 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0234
• Residual factor for significantly intense reflections: 0.0233
• Weighted residual factors for all reflections: 0.0634
• Weighted residual factors for significantly intense reflections: 0.0633
• Goodness-of-fit parameter for all reflections: 1.185
• Goodness-of-fit parameter for significantly intense reflections: 1.185
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No