Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4323372
Preview
Coordinates | 4323372.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | [SP-4-4-[(R~C~),(R~P~,R~P~)]]-bis[1-[1-dimethylamino)ethyl]-2-phenyl- C^2^,N](1,1,4,7,10,10-hexaphenyl-1,4,7,10-tetraphosphadecane- P,P,P,P)dipalladium(II) hexafluorophosphate |
---|---|
Formula | C62 H70 F12 N2 P6 Pd2 |
Calculated formula | C62 H70 F12 N2 P6 Pd2 |
Title of publication | Self-Assembly of Homochiral Double Helix and Side-by-Side Helix Conformers of Double-Stranded Disilver(I)- and Digold(I)-Tetra(tertiary phosphine) Helicates |
Authors of publication | Anthea L. Airey; Gerhard F. Swiegers; Anthony C. Willis; S. Bruce Wild |
Journal of publication | Inorganic Chemistry |
Year of publication | 1997 |
Journal volume | 36 |
Pages of publication | 1588 - 1597 |
a | 10.841 ± 0.003 Å |
b | 13.668 ± 0.002 Å |
c | 22.33 ± 0.003 Å |
α | 90° |
β | 103.09 ± 0.01° |
γ | 90° |
Cell volume | 3222.8 ± 1.1 Å3 |
Cell temperature | 293 K |
Ambient diffraction temperature | 293 K |
Number of distinct elements | 6 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.054 |
Residual factor for significantly intense reflections | 0.036 |
Weighted residual factors for all reflections | 0.039 |
Weighted residual factors for significantly intense reflections | 0.034 |
Goodness-of-fit parameter for all reflections | 2.01 |
Goodness-of-fit parameter for significantly intense reflections | 2.043 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4323372.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.