Information card for entry 4323392

Structure parameters

• Formula: C43 H74 N6 Pb3 Sb2
• Calculated formula: C43 H74 N6 Pb3 Sb2
• SMILES: [Pb]123[N]4(C5CCCCC5)[Pb]56[N]7(C8CCCCC8)[Sb]([N]1(C1CCCCC1)[Pb]17[N]6(C6CCCCC6)[Sb]4[N]21C1CCCCC1)[N]35C1CCCCC1.Cc1ccccc1
• Title of publication: Assembly of Mixed-Metal Cages Using Polyimido Antimony(III) Anions. Syntheses and Structures of [Sb3(NCy)4(HNCy)2]K.2(toluene), [Sb2(NCy)4]2M4 (M = Cu, Ag), and [Sb(NCy)3]2Pb3 (Cy = Cyclohexyl, C6H11)
• Authors of publication: Michael A. Beswick; Natalie L. Cromhout; Christopher N. Harmer; Michael A. Paver; Paul R. Raithby; Moira-Ann Rennie; Alexander Steiner; Dominic S. Wright
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 1740 - 1744
• a: 11.071 ± 0.002 Å
• b: 14.892 ± 0.003 Å
• c: 17.262 ± 0.003 Å
• α: 65.36 ± 0.03°
• β: 74.21 ± 0.03°
• γ: 70.7 ± 0.03°
• Cell volume: 2411.3 ± 1 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1337
• Residual factor for significantly intense reflections: 0.0909
• Weighted residual factors for all reflections: 0.2961
• Weighted residual factors for significantly intense reflections: 0.237
• Goodness-of-fit parameter for all reflections: 1.063
• Goodness-of-fit parameter for significantly intense reflections: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No