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Information card for entry 4323402
Preview
Coordinates | 4323402.cif |
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Original paper (by DOI) | HTML |
Formula | C52 H96 Ag4 N8 O Sb4 |
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Calculated formula | C52 H96 Ag4 N8 O Sb4 |
Title of publication | Assembly of Mixed-Metal Cages Using Polyimido Antimony(III) Anions. Syntheses and Structures of [Sb3(NCy)4(HNCy)2]K.2(toluene), [Sb2(NCy)4]2M4 (M = Cu, Ag), and [Sb(NCy)3]2Pb3 (Cy = Cyclohexyl, C6H11) |
Authors of publication | Michael A. Beswick; Natalie L. Cromhout; Christopher N. Harmer; Michael A. Paver; Paul R. Raithby; Moira-Ann Rennie; Alexander Steiner; Dominic S. Wright |
Journal of publication | Inorganic Chemistry |
Year of publication | 1997 |
Journal volume | 36 |
Pages of publication | 1740 - 1744 |
a | 11.501 ± 0.002 Å |
b | 13.752 ± 0.003 Å |
c | 22.868 ± 0.005 Å |
α | 103.5 ± 0.03° |
β | 95.89 ± 0.03° |
γ | 96.71 ± 0.03° |
Cell volume | 3461.1 ± 1.4 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0791 |
Residual factor for significantly intense reflections | 0.0513 |
Weighted residual factors for all reflections | 0.2832 |
Weighted residual factors for significantly intense reflections | 0.174 |
Goodness-of-fit parameter for all reflections | 1.109 |
Goodness-of-fit parameter for significantly intense reflections | 0.795 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4323402.html
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