Information card for entry 4323408

Structure parameters

• Formula: C18 H45 Cl3 N8 Ni O13
• Calculated formula: C18 H45 Cl3 N8 Ni O16
• Title of publication: A Loose Cage for Transition Metals
• Authors of publication: Giancarlo De Santis; Luigi Fabbrizzi; Angelo Perotti; Nicola Sardone; Angelo Taglietti
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 1998 - 2003
• a: 14.173 ± 0.002 Å
• b: 14.383 ± 0.001 Å
• c: 30.622 ± 0.003 Å
• α: 90 ± 0°
• β: 90 ± 0°
• γ: 90 ± 0°
• Cell volume: 6242.3 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for significantly intense reflections: 0.049
• Weighted residual factors for significantly intense reflections: 0.054
• Goodness-of-fit parameter for significantly intense reflections: 2.51
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No