Information card for entry 4323424

Structure parameters

• Formula: C35 H58 N6 O15 V4
• Calculated formula: C35 H58 N6 O15 V4
• Title of publication: Competing Magnetic Exchange Interactions in Tetranuclear d^1^ Systems: Synthesis, Structure, and Magnetochemistry of a Neutral Vanadium(IV) Complex with a {(VO)4(μ3-OR)2(μ2-OR)4}2+ Core
• Authors of publication: Winfried Plass
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 2200 - 2205
• a: 7.352 ± 0.002 Å
• b: 12.584 ± 0.004 Å
• c: 12.826 ± 0.004 Å
• α: 107.61 ± 0.02°
• β: 102.96 ± 0.02°
• γ: 95.25 ± 0.02°
• Cell volume: 1085.9 ± 0.6 ų
• Cell temperature: 188 ± 2 K
• Ambient diffraction temperature: 188 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1348
• Residual factor for significantly intense reflections: 0.0712
• Weighted residual factors for all reflections: 0.1861
• Weighted residual factors for significantly intense reflections: 0.1517
• Goodness-of-fit parameter for all reflections: 1.012
• Goodness-of-fit parameter for significantly intense reflections: 1.118
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No