Information card for entry 4323475

Structure parameters

• Common name: compound 4
• Formula: C21 H27 Cl N2 Sb
• Calculated formula: C21 H27 Cl N2 Sb
• Title of publication: Synthesis and Structures of Intramolecularly Base-Coordinated Group 15 Aryl Halides
• Authors of publication: Claire J. Carmalt; Alan H. Cowley; Robert D. Culp; Richard A. Jones; Smuruthi Kamepalli; Nicholas C. Norman
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 2770 - 2776
• a: 9.1483 ± 0.0011 Å
• b: 9.4868 ± 0.0011 Å
• c: 12.9776 ± 0.0012 Å
• α: 70.614 ± 0.008°
• β: 85.738 ± 0.009°
• γ: 83.094 ± 0.009°
• Cell volume: 1054 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1302
• Residual factor for significantly intense reflections: 0.042
• Weighted residual factors for all reflections: 0.0852
• Weighted residual factors for significantly intense reflections: 0.0647
• Goodness-of-fit parameter for all reflections: 1.044
• Goodness-of-fit parameter for significantly intense reflections: 1.093
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No