Information card for entry 4323499

Structure parameters

• Formula: C64 H32 Bi2 F40 Na4 O13
• Calculated formula: C64 H32 Bi1.998 F40 Na4.002 O13
• Title of publication: Oligomerization and Oxide Formation in Bismuth Aryloxides: Synthesis, Characterization, and Structures of [NaBi(OC6F5)4(THF)]∞and Na4Bi2(μ6-O)(OC6F5)8(THF)4
• Authors of publication: Jennifer L. Jolas; Silke Hoppe; Kenton H. Whitmire
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 3335 - 3340
• a: 14.059 ± 0.003 Å
• b: 14.06 ± 0.003 Å
• c: 11.531 ± 0.002 Å
• α: 108.47 ± 0.03°
• β: 102.78 ± 0.03°
• γ: 108.61 ± 0.03°
• Cell volume: 1912.6 ± 1.1 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1335
• Residual factor for significantly intense reflections: 0.0833
• Weighted residual factors for all reflections: 0.2296
• Weighted residual factors for significantly intense reflections: 0.2
• Goodness-of-fit parameter for all reflections: 1.066
• Goodness-of-fit parameter for significantly intense reflections: 1.11
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No