Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4323510
Preview
Coordinates | 4323510.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C51 H45 Cl P2 Pd |
---|---|
Calculated formula | C51 H45 Cl P2 Pd |
Title of publication | A Bidentate Bisphosphine Functioning in Intramolecular Aliphatic Metalation and as an NMR Spectroscopic Probe for the Metal Coordination Environment |
Authors of publication | William Lesueur; Euro Solari; Carlo Floriani; Angiola Chiesi-Villa; Corrado Rizzoli |
Journal of publication | Inorganic Chemistry |
Year of publication | 1997 |
Journal volume | 36 |
Pages of publication | 3354 - 3362 |
a | 11.289 ± 0.001 Å |
b | 18.769 ± 0.002 Å |
c | 11.077 ± 0.001 Å |
α | 91.2 ± 0.01° |
β | 110.27 ± 0.01° |
γ | 105.26 ± 0.01° |
Cell volume | 2107.7 ± 0.4 Å3 |
Cell temperature | 25 K |
Ambient diffraction temperature | 295 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0399 |
Residual factor for significantly intense reflections | 0.0387 |
Weighted residual factors for all reflections | 0.1124 |
Weighted residual factors for significantly intense reflections | 0.1025 |
Goodness-of-fit parameter for all reflections | 1.021 |
Goodness-of-fit parameter for significantly intense reflections | 1.021 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4323510.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.