Information card for entry 4323539

Structure parameters

• Formula: C24 H34 Cl3 O2 Ta
• Calculated formula: C26 H40 Cl3 O2 Ta
• Title of publication: Structural Distortions in Six-Coordinate Adducts of Niobium(V) and Tantalum(V)
• Authors of publication: Janet R. Clark; April L. Pulvirenti; Phillip E. Fanwick; Michaelis Sigalas; Odile Eisenstein; Ian P. Rothwell
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 3623 - 3631
• a: 12.757 ± 0.006 Å
• b: 15.558 ± 0.009 Å
• c: 13.625 ± 0.009 Å
• α: 90°
• β: 90.83 ± 0.06°
• γ: 90°
• Cell volume: 2704 ± 3 ų
• Cell temperature: 297 K
• Ambient diffraction temperature: 297 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.188
• Residual factor for significantly intense reflections: 0.072
• Weighted residual factors for all reflections: 0.242
• Weighted residual factors for significantly intense reflections: 0.16
• Goodness-of-fit parameter for all reflections: 1.109
• Goodness-of-fit parameter for significantly intense reflections: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No