Information card for entry 4323542

Structure parameters

• Formula: C32 H45 Cl3 Nb O2 P
• Calculated formula: C32 H45 Cl3 Nb O2 P
• Title of publication: Structural Distortions in Six-Coordinate Adducts of Niobium(V) and Tantalum(V)
• Authors of publication: Janet R. Clark; April L. Pulvirenti; Phillip E. Fanwick; Michaelis Sigalas; Odile Eisenstein; Ian P. Rothwell
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 3623 - 3631
• a: 19.153 ± 0.004 Å
• b: 17.372 ± 0.005 Å
• c: 10.461 ± 0.008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3481 ± 3 ų
• Cell temperature: 297 K
• Ambient diffraction temperature: 297 K
• Number of distinct elements: 6
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.23
• Residual factor for significantly intense reflections: 0.062
• Weighted residual factors for all reflections: 0
• Weighted residual factors for significantly intense reflections: 0.114
• Goodness-of-fit parameter for all reflections: 0
• Goodness-of-fit parameter for significantly intense reflections: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No