Information card for entry 4323545

Structure parameters

• Formula: C50 H69 Cl3 Nb O3 P
• Calculated formula: C50 H69 Cl3 Nb O3 P
• Title of publication: Structural Distortions in Six-Coordinate Adducts of Niobium(V) and Tantalum(V)
• Authors of publication: Janet R. Clark; April L. Pulvirenti; Phillip E. Fanwick; Michaelis Sigalas; Odile Eisenstein; Ian P. Rothwell
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 3623 - 3631
• a: 10.505 ± 0.002 Å
• b: 12.967 ± 0.004 Å
• c: 19.289 ± 0.003 Å
• α: 83.174 ± 0.019°
• β: 89.352 ± 0.015°
• γ: 89.2 ± 0.02°
• Cell volume: 2608.5 ± 1 ų
• Cell temperature: 295 K
• Ambient diffraction temperature: 295 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.134
• Residual factor for significantly intense reflections: 0.046
• Weighted residual factors for significantly intense reflections: 0.052
• Goodness-of-fit parameter for significantly intense reflections: 1.351
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No