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Information card for entry 4323556
Preview
Coordinates | 4323556.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C50 H38 Cl4 Ge N4 O4 |
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Calculated formula | C50 H38 Cl4 Ge N4 O4 |
Title of publication | Molecular Structures of Ge(tpp)(OAc)2and In(tpp)(OAc) and Their Implications: Correlations between the 13C NMR Chemical Shift of the Acetato Ligand and Different Types of Carboxylate Coordination in M(por)(OAc)n {por = tpp (5,10,15,20-Tetraphenylporphyrinate), tmpp (5,10,15,20-Tetrakis(4-methoxyphenyl)porphyrinate), tpyp (5,10,15,20-Tetrakis(4-pyridyl)porphyrinate); M = Ga, In, Tl, Ge, Sn; n= 1, 2} |
Authors of publication | Shwu-Juian Lin; Tay-Ning Hong; Jo-Yu Tung; Jyh-Horung Chen |
Journal of publication | Inorganic Chemistry |
Year of publication | 1997 |
Journal volume | 36 |
Pages of publication | 3886 - 3891 |
a | 10.167 ± 0.002 Å |
b | 11.358 ± 0.002 Å |
c | 11.672 ± 0.002 Å |
α | 61.52 ± 0.01° |
β | 74.5 ± 0.01° |
γ | 74.3 ± 0.01° |
Cell volume | 1125.2 ± 0.4 Å3 |
Cell temperature | 293 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for significantly intense reflections | 0.077 |
Weighted residual factors for significantly intense reflections | 0.098 |
Goodness-of-fit parameter for significantly intense reflections | 1.29 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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