Information card for entry 4323582

Structure parameters

• Formula: C21 H10 N2 O10 Os3 S2
• Calculated formula: C21 H10 N2 O10 Os3 S2
• Title of publication: Reactions of Triosmium Carbonyl Clusters with Thionylaniline. Crystal Structures of Os~3~(CO)~9~(μ~3~-NPh)(μ~3~-S), Os~3~(CO)~9~(μ~3~,η^2^-(PhN)~2~SO)(μ~3~-S), and Os~3~(CO)~8~(NCMe)(μ~3~-NPh)(μ~3~-S).
• Authors of publication: Wen-Yann Yeh; Charlotte L. Stern; Duward F. Shriver
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 4408 - 4414
• a: 9.723 ± 0.004 Å
• b: 15.704 ± 0.004 Å
• c: 18.455 ± 0.007 Å
• α: 113.17 ± 0.03°
• β: 102.48 ± 0.03°
• γ: 89.97 ± 0.03°
• Cell volume: 2518.2 ± 1.7 ų
• Cell temperature: 153.2 K
• Ambient diffraction temperature: 153.2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0298
• Weighted residual factors for significantly intense reflections: 0.0255
• Goodness-of-fit parameter for significantly intense reflections: 1.312
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No