Information card for entry 4323590

Structure parameters

• Formula: C50 H40 Cl F10 N4 O4 P Pd2
• Calculated formula: C50 H26 Cl F10 N4 O4 P Pd2
• Title of publication: Synthesis, Molecular Structure, and Reactivity of the Tetranuclear Complex [NBu4]2[Pd4(μ-PPh2)2(μ-Cl)4(C6F5)4]. Molecular Structure of [Pd2(μ-PPh2)(C6F5)2(bipy)2]ClO4.C6H14
• Authors of publication: Ester Alonso; Juan Forniés; Consuelo Fortuño; Antonio Martín; Georgina M. Rosair; Alan J. Welch
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 4426 - 4431
• a: 16.214 ± 0.003 Å
• b: 10.311 ± 0.002 Å
• c: 28.38 ± 0.006 Å
• α: 90°
• β: 100.82 ± 0.03°
• γ: 90°
• Cell volume: 4660.3 ± 1.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0698
• Residual factor for significantly intense reflections: 0.0398
• Weighted residual factors for all reflections: 0.0875
• Weighted residual factors for significantly intense reflections: 0.0829
• Goodness-of-fit parameter for all reflections: 0.846
• Goodness-of-fit parameter for significantly intense reflections: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No