Information card for entry 4323592

Structure parameters

• Formula: C67 H69 Au3 F3 O14 P3 S
• Calculated formula: C67 H63 Au3 F3 O14 P3 S
• Title of publication: Gold(I) Complexes with N-Donor Ligands. 2.1 Reactions of Ammonium Salts with [Au(acac-κC2)(PR3)] To Give [Au(NH3)L]+, [(AuL)2(μ2-NH2)]+, [(AuL)4(μ4-N)]+, or [(AuL)3(μ3-O)]+. A New and Facile Synthesis of [Au(NH3)2]+Salts. Crystal Structure of [{AuP(C6H4OMe-4)3}3(μ3-O)]CF3SO3
• Authors of publication: José Vicente; María-Teresa Chicote; Rita Guerrero; Peter G. Jones; M. Carmen Ramírez de Arellano
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 4438 - 4443
• a: 14.884 ± 0.003 Å
• b: 15.828 ± 0.003 Å
• c: 16.061 ± 0.003 Å
• α: 83.39 ± 0.03°
• β: 86.28 ± 0.03°
• γ: 65.54 ± 0.03°
• Cell volume: 3420.6 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0464
• Residual factor for significantly intense reflections: 0.037
• Weighted residual factors for all reflections: 0.0869
• Weighted residual factors for significantly intense reflections: 0.0788
• Goodness-of-fit parameter for all reflections: 1.043
• Goodness-of-fit parameter for significantly intense reflections: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No